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HRID2394287

反应详情

EQUATION

反应方程式

HRID 2394287 的结构方程式

REACTANTS

反应物

2
结构：O=C([O-])[O-].[K+].[K+]
HCID11430

Potassium Carbonate

CK2O3

结构：CCOC(=O)C(=CNC1CC1)C(=O)c1cnc(Cl)c(Cl)c1Cl
HCID178471896

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1cn(C2CC2)c2c(Cl)c(Cl)ncc2c1=O
HCID15334456

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

17.5 g (0.048 mol) of ethyl 2-(4,5,6-trichloronicotinoyl)-3-cyclopropylamino-acrylate are heated with 7.7 g (0.056 mol) of potassium carbonate in 100 ml of DMF at 60° C. for two hours. Ice-water is added to the cooled mixture, and the product is isolated.

WORKUP

后处理

  1. customthe product is isolated