HRID2394484

反应详情

EQUATION

反应方程式

HRID 2394484 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Benzaldehyde (2-hydroxyethyl)hydrazone is prepared by condensation of benzaldehyde with (2-hydroxyethyl)hydrazine according to the following procedure: 10-2 moles of (2-hydroxyethyl)hydrazine are added to a solution containing 10-2 moles of benzaldehyde in 20 ml of ethanol. The reaction is left under reflux for 30 minutes. The mixture is then cooled. The solvents are removed by evaporation. The product obtained is an extremely unstable oil. The crude reaction yield is 97%.

WORKUP

后处理

  1. waitThe reaction is left
  2. temperatureunder reflux for 30 minutes
  3. temperatureThe mixture is then cooled
  4. customThe solvents are removed by evaporation
  5. customThe product obtained
  6. customThe crude reaction yield is 97%