Potassium Carbonate → HCID 21435290, compound

HRID 2398474Notes

Reaction equation

HRID 2398474 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[C:12]3[CH:13]=[CH:14][CH:15]=[CH:16][C:11]=3[O:10][C:9]=2[C:17](=[O:25])[C:18]2[CH:23]=[CH:22][C:21]([OH:24])=[CH:20][CH:19]=2)=[CH:4][CH:3]=1.[CH2:26]([N:28]([CH2:33][CH3:34])[CH2:29][CH2:30][CH2:31]Cl)[CH3:27].C(=O)([O-])[O-].[K+].[K+]>CCC(=O)CC>[Cl:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2[C:12]3[CH:13]=[CH:14][CH:15]=[CH:16][C:11]=3[O:10][C:9]=2[C:17](=[O:25])[C:18]2[CH:19]=[CH:20][C:21]([O:24][CH2:31][CH2:30][CH2:29][N:28]([CH2:33][CH3:34])[CH2:26][CH3:27])=[CH:22][CH:23]=2)=[CH:6][CH:7]=1

Participants

5

Reactant 3

HCID 11430Potassium CarbonateHCID 669183-Chloropropyl(diethyl)amineHCID 21435341[3-(4-Chlorophenyl)-1-benzofuran-2-yl](4-hydroxyphenyl)methanone

Product 1

HCID 21435290HCID 21435290, compound

Reagents, catalysts & solvents 1

HCID 7288Ethyl ketoneSolvent

Procedure

(0.009 mol.) of 3-(4-chlorophenyl)-2-(4-hydroxybenzoyl)benzofuran with 1.4 g. (0.009 mol.) of 3-diethylaminopropyl chloride in 50 ml. of dry 3-pentanone containing 5.2 g. (0.04 mol.) of potassium carbonate by the method described in Example 1 gives the title compound.

Sources & evidence

ORD record
ord-20db93eb3a2942f2941cdf421ce5d9e9
Source dataset
uspto-grants-1977_05
Patent number
US04024273

Reaction notes

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