HRID2399124

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID68284

Benzoyl isothiocyanate

C8H5NOS

HCID12889401

2-[(2-Pyridinylmethyl)thio]ethanamine

C8H12N2S

PRODUCTS

生成物

HCID21432770

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID6212

Chloroform

CHCl3

PROCEDURE

实验过程

A solution of 2-[(2-aminoethyl)thiomethyl]pyridine (6.0 g.) and benzoyl isothiocyanate (6.0 g.) in chloroform (150 ml.) is heated under reflux for one hour and concentrated to give N-benzoyl-N'-[2-(2-pyridylmethylthio)ethyl]thiourea.

WORKUP

后处理

temperatureunder reflux for one hour
concentrationconcentrated