HRID2399383

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID5362487

Sulfur

HCID53884445

Acetic acid, 2-(3,4-dihydro-7-methoxy-1(2H)-naphthalenylidene)-, ethyl ester

C15H18O3

PRODUCTS

生成物

HCID13570063

Ethyl (7-methoxynaphthalen-1-yl)acetate

C15H16O3

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8857

Ethyl acetate

C4H8O2

CONDITIONS

反应条件

温度: 215 °C

PROCEDURE

实验过程

50 g of ethyl 7-methoxy-1,2,3,4-tetrahydro-1-naphthylideneacetate are mixed with 7.35 g of sulphur, and the mixture is heated at 215° C. for 10 hours. It is cooled, 300 cm3 of ethyl acetate are added, and the mixture is stirred for 30 minutes and filtered. It is then dried.

WORKUP

后处理

temperatureIt is cooled
filtrationfiltered
customIt is then dried