HRID240606

反应详情

EQUATION

反应方程式

HRID 240606 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

4-(5-Fluoro-2-nitrophenoxy)tetrahydro-2-H-pyran (8.4 g) was dissolved in ethylacetate (30 ml) and Pd/C (500 mg) was added. The reaction was hydrogenated at room temperature and 50 PSI. The mixture was concentrated in vacuo to give the intended product.

WORKUP

后处理

  1. customwas hydrogenated at room temperature
  2. concentrationThe mixture was concentrated in vacuo
  3. customto give the intended product