HRID2406643

反应详情

EQUATION

反应方程式

HRID 2406643 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a solution of 2-undecyl-1H-indole in DMSO was added KOH at RT and was stirred for 30 minutes. Then to this mixture was dihydro-pyran-2,6-dione and stirred for 3 hours. The reaction mixture was treated with saturated ammonium chloride and ethyl acetate. The product was purified by column chromatography.

WORKUP

后处理

  1. stirringstirred for 3 hours
  2. customThe product was purified by column chromatography