反应详情

温度

0 °C

[3-(t-Butyl-dimethyl-silanyloxy)-azetidin-1-yl]-carbamic acid t-butyl ester (100 mg, 331 mmol) was at 0° C. combined with trifluoroacetic acid (2 mL) to give a colorless solution. The reaction mixture was stirred for 2 h at 0° C. and subsequently concentrated in vacuo to give the title compound as colorless oil, which was used without further purification in the next step.

1. customwas at 0° C.
2. customto give a colorless solution
3. concentrationsubsequently concentrated in vacuo