反应详情

5-Bromogramine, 60.0 g., 165 g. of 2-nitropropane, and 10.5 g. of sodium hydroxide pellets were caused to react under the conditions of Procedure 10C. The product was recovered as a dark syrup-like liquid from which the crystalline product was obtained by dissolving in i-Pr2O. The crystalline material was recrystallized from i-Pr2O to yield 48.6 g. of tan crystalline product, m.p. 106°-109°. The structure was confirmed by examination of the NMR spectrum.

1. customto react under the conditions of Procedure 10C
2. customThe product was recovered as a dark syrup-like liquid from which the crystalline product
3. customwas obtained
4. customThe crystalline material was recrystallized from i-Pr2O
5. customto yield 48.6 g