HRID2413498

反应详情

EQUATION

反应方程式

HRID 2413498 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

22.1 g of N-(4-chlorophenyl)-3-methoxyphenylacetamide are reduced with lithium aluminum hydride in THF. After destroying the reagent with water, filtering, drying and evaporating in a rotary evaporator, the oily residue is taken up in diethyl ether, and the desired product is precipitated as the hydrochloride.

WORKUP

后处理

  1. customAfter destroying the reagent with water
  2. filtrationfiltering
  3. customdrying
  4. customevaporating in a rotary evaporator
  5. customthe desired product is precipitated as the hydrochloride