Butyl iodide → HCID 86234905, compound

HRID 2414115Notes

Reaction equation

HRID 2414115 reaction equation
[Na][Na].[C:3]([NH:5][C:6](=[O:16])[CH2:7][CH2:8][CH2:9][CH2:10][C:11]([NH:13][C:14]#[N:15])=[O:12])#[N:4].[CH2:17](I)[CH2:18][CH2:19][CH3:20]>CN1CCCC1=O>[C:14]([N:13]([CH2:6][CH2:7][CH2:8][CH3:9])[C:11](=[O:12])[CH2:10][CH2:9][CH2:8][CH2:7][C:6]([N:5]([CH2:17][CH2:18][CH2:19][CH3:20])[C:3]#[N:4])=[O:16])#[N:15]

Participants

5

Reactant 3

HCID 10962Butyl iodideHCID 141233DisodiumHCID 3015775N,N'-Dicyanoadipamide

Product 1

HCID 86234905HCID 86234905, compound

Reagents, catalysts & solvents 1

HCID 13387N-methyl-2-pyrrolidoneSolvent

Procedure

Analogously to Example 3, 23.8 g (0.1 mol) of the disodium salt of adipic acid bis-(N-cyanamide) and 55.2 g (0.2 mol+50% excess) of n-butyl iodide are reacted in 50 ml of N-methylpyrrolidone at 92°-100° C. for 5 hours and 15 minutes and the mixture is worked up.

Sources & evidence

ORD record
ord-08455c6dce874b1186a7be0c42baafd5
Source dataset
uspto-grants-1988_01
Patent number
US04721770

Reaction notes

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