HRID2414300

反应详情

EQUATION

反应方程式

HRID 2414300 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A suspension was prepared of 46.5 g of 1-acetyloxy-2-(3-methoxyphenyl)-6-methoxynaphthalene and 40 mL of 5N HCl in 400 mL of MeOH. The reaction mixture was heated to reflux for eleven hours. The reaction mixture was evaporated to a clear oil. This yielded 38.6 g of the title compound.

WORKUP

后处理

  1. temperatureThe reaction mixture was heated
  2. temperatureto reflux for eleven hours
  3. customThe reaction mixture was evaporated to a clear oil