Triethylamine → HCID 69669790, compound

HRID 241603Notes

Reaction equation

HRID 241603 reaction equation
[N:1]1([CH2:6][C:7]([O:9][CH2:10]C)=[O:8])[CH:5]=[CH:4][N:3]=[N:2]1.[CH2:12](N(CC)CC)C>CO>[N:1]1([C:6](=[CH2:12])[C:7]([O:9][CH3:10])=[O:8])[CH:5]=[CH:4][N:3]=[N:2]1

Participants

4

Reactant 2

HCID 8471TriethylamineHCID 10103365ETHYL 2-(1H-1,2,3-TRIAZOL-1-YL)ACETATE

Product 1

HCID 69669790HCID 69669790, compound

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Conditions

Temperature
22 °C

Procedure

450 g of ethyl 2-(1H-1,2,3-triazol-1-yl)acetate were dissolved in 3.5 1 of methanol, 30 g of triethylamine were added and the mixture was stirred at 22° C. for 16 h. All solvents were then distilled off under reduced pressure. This gave 410 g of the title compound as an oil.

Workup

  1. additionwere added
  2. distillationAll solvents were then distilled off under reduced pressure

Sources & evidence

ORD record
ord-a65d5812e32c46648999775e580451ae
Source dataset
uspto-grants-2014_02
Patent number
US08653074B2

Reaction notes

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