6-Chloro-2-pyridinol → 1355729-47-3

HRID 2418862Notes

Reaction equation

HRID 2418862 reaction equation
O=S(O)C(F)F.O=c1cccc(Cl)[nH]1.[Zn]>CC(C)(C)OO.ClCCl.O.O=C(O)C(F)(F)F>O=c1ccc(C(F)F)c(Cl)[nH]1

Participants

7

Reactant 2

HCID 856216-Chloro-2-pyridinolHCID 89600919CID 89600919

Product 1

HCID 896097151355729-47-3Yield 62%

Reagents, catalysts & solvents 4

HCID 6410tert-Butyl hydroperoxideReagentHCID 6422Trifluoroacetic acidReagentHCID 962WaterSolventHCID 6344DichloromethaneSolvent

Conditions

Temperature
25 °C

Sources & evidence

ORD record
ord-ae369c45f8f641fc99ab7038230d1e29
Source dataset
Minisci dataset from Roche

Reaction notes

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