Hydrochloric Acid → HCID 178479327, compound

HRID 2419781Notes

Reaction equation

HRID 2419781 reaction equation
[CH2:1]([NH:8][C:9]([NH:11][N:12]=[CH:13][C:14]1[C:19]([Cl:20])=[CH:18][CH:17]=[CH:16][C:15]=1[Cl:21])=[NH:10])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.C(O)C.Cl>C(O)(C)C>[ClH:20].[CH2:1]([NH:8][C:9]([NH:11][N:12]=[CH:13][C:14]1[C:15]([Cl:21])=[CH:16][CH:17]=[CH:18][C:19]=1[Cl:20])=[NH:10])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 702EthanolHCID 178512100HCID 178512100, compound

Product 1

HCID 178479327HCID 178479327, compound

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

To a solution of 2.00 g. of 1-benzyl-3-(2,6-dichlorobenzylideneamino)guanidine in 40 ml. of absolute ethanol is added 20 ml. of 3.75 N hydrogen chloride in isopropyl alcohol. The mixture is evaporated under reduced pressure, giving the desired product as a colorless solid, m.p. 58°-68° C.

Workup

  1. customThe mixture is evaporated under reduced pressure

Sources & evidence

ORD record
ord-51c9b6a8b9e44cc0bf9c49bbd452d737
Source dataset
uspto-grants-1978_08
Patent number
US04107326

Reaction notes

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