HRID2421031

反应详情

EQUATION

反应方程式

HRID 2421031 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A suspension of ethyl 6-oxo-2-(pentafluoroethyl)-1,6-dihydropyridine-3-carboxylate (0.300 g) in concentrated hydrochloric acid (10 mL) was heated at reflux for 20 h. The reaction mixture was cooled and a colourless solid filtered off (0.30 g).

WORKUP

后处理

  1. temperaturewas heated
  2. temperatureat reflux for 20 h
  3. temperatureThe reaction mixture was cooled
  4. filtrationa colourless solid filtered off (0.30 g)