4-Hydroxybenzaldehyde → HCID 11545644, compound

HRID 2422649Notes

Reaction equation

HRID 2422649 reaction equation
[NH2:1][C:2]1[C:10]([O:11][CH3:12])=[CH:9][CH:8]=[CH:7][C:3]=1[C:4]([OH:6])=O.[CH3:13][NH2:14].[OH:15][C:16]1[CH:23]=[CH:22][C:19]([CH:20]=O)=[CH:18][CH:17]=1.[Br-].Br[CH2:26][CH2:27][CH2:28][NH+:29]1[CH2:33][CH2:32][CH2:31][CH2:30]1>>[CH3:12][O:11][C:10]1[CH:9]=[CH:8][CH:7]=[C:3]2[C:2]=1[N:1]=[C:20]([C:19]1[CH:22]=[CH:23][C:16]([O:15][CH2:26][CH2:27][CH2:28][N:29]3[CH2:33][CH2:32][CH2:31][CH2:30]3)=[CH:17][CH:18]=1)[N:14]([CH3:13])[C:4]2=[O:6]

Participants

5

Reactant 4

HCID 1264-HydroxybenzaldehydeHCID 6329MethylamineHCID 2557202-Amino-3-methoxybenzoic acidHCID 178419552HCID 178419552, compound

Product 1

HCID 11545644HCID 11545644, compound

Procedure

The entitled compound was obtained according to the method of Example 77 but using 2-amino-3-methoxybenzoic acid, methylamine, 4-hydroxybenzaldehyde and 1-(3-bromopropyl)pyrrolidinium bromide.

Workup

  1. customThe entitled compound was obtained

Sources & evidence

ORD record
ord-82551cce29cf4538baa81f77573a2c44
Source dataset
uspto-grants-2011_06
Patent number
US07960394B2

Reaction notes

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