Anthranilic Acid → HCID 11682287, compound

HRID 2422655Notes

Reaction equation

HRID 2422655 reaction equation
[C:1]([OH:10])(=O)[C:2]1[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=1)[NH2:4].[CH3:11][NH2:12].[CH3:13][O:14][C:15]1[CH:22]=[CH:21][C:18]([CH:19]=O)=[CH:17][CH:16]=1.OC1[CH2:29][CH2:28][N:27](C(OC(C)(C)C)=O)[CH2:26][CH2:25]1.C(O[C:40]1(O[Si](C)(C)C)[CH2:42][CH2:41]1)C>>[CH3:11][N:12]1[C:1](=[O:10])[C:2]2[C:3](=[CH:5][CH:6]=[CH:7][CH:8]=2)[N:4]=[C:19]1[C:18]1[CH:21]=[CH:22][C:15]([O:14][CH:13]2[CH2:29][CH2:28][N:27]([CH:40]3[CH2:41][CH2:42]3)[CH2:26][CH2:25]2)=[CH:16][CH:17]=1

Participants

6

Reactant 5

HCID 227Anthranilic AcidHCID 6329MethylamineHCID 312444-MethoxybenzaldehydeHCID 643502Tert-butyl 4-hydroxypiperidine-1-carboxylateHCID 2734686(1-Ethoxycyclopropoxy)trimethylsilane

Product 1

HCID 11682287HCID 11682287, compound

Procedure

The entitled compound was obtained according to the method of Example 85 but using anthranilic acid, methylamine, 4-methoxybenzaldehyde, tert-butyl 4-hydroxytetrahydro-1(2H)-pyridinecarboxylate, and [(1-ethoxycyclopropyl)oxy](trimethyl)silane.

Workup

  1. customThe entitled compound was obtained

Sources & evidence

ORD record
ord-4a7550e31c6d4c8aae85c8ca7c6416ee
Source dataset
uspto-grants-2011_06
Patent number
US07960394B2

Reaction notes

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