HRID242267

反应详情

EQUATION

反应方程式

HRID 242267 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

250 mg (1.19 mmol) of the compound from Example 3A, 122 mg (0.99 mmol) of the compound from Example 1A and 23 mg (99 μmol) camphor-10-sulfonic acid are dissolved in 5 ml anhydrous ethanol and the mixture is heated under reflux overnight.

WORKUP

后处理

  1. temperaturethe mixture is heated
  2. temperatureunder reflux overnight