HRID244610

反应详情

EQUATION

反应方程式

HRID 244610 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

6-(1H-Indol-4-yl)-4-nitro-2-(tetrahydro-2H-pyran-2-yl)-2H-indazole (2.54 g), ethyl acetate (100 ml) and 10% palladium on carbon (250 mg) were placed under an atmosphere of hydrogen and the mixture stirred overnight. The mixture was filtered through Celite and the solvent removed in vacuo to give the title compound as an off white solid (2.27 g).

WORKUP

后处理

  1. filtrationThe mixture was filtered through Celite
  2. customthe solvent removed in vacuo