反应详情

Dibenzylamine (39.4 g, 0.20 mol) was added to 100 mL of methylene dichloride and stirred for 30 minutes. (S)-epichlorohydrin (21 g, 0.23 mol) was then added. The mixture was stirred at room temperature (25° C.) for 20 hours. Filtered, and the solvent was evaporated to provide 55 g of colorless oil in 93% yield.

1. stirringThe mixture was stirred at room temperature (25° C.) for 20 hours
2. filtrationFiltered
3. customthe solvent was evaporated