Hydrochloric Acid → HCID 13532852, compound

HRID 247623Notes

Reaction equation

HRID 247623 reaction equation
[ClH:1].[CH:2]1([NH2:9])[CH2:8][CH2:7][CH2:6][CH2:5][CH:4]=[CH:3]1>C(O)(C)C>[ClH:1].[CH:2]1([NH2:9])[CH2:8][CH2:7][CH2:6][CH2:5][CH:4]=[CH:3]1

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 11263481Cyclohept-2-en-1-amine

Product 1

HCID 13532852HCID 13532852, compoundYield 94.8%

Reagents, catalysts & solvents 1

HCID 3776IsopropanolSolvent

Procedure

Conc. hydrochloric acid (10.1 g) was added dropwise to a mixture of 2-cycloheptenylamine (11.1 g, 0.1 mole) and isopropyl alcohol (24 g) with stirring and ice-cooling. The reaction mixture was concentrated under reduced pressure, and the deposited crystal was washed with diethyl ether and dried to obtain 14 g of 2-cycloheptenylamine hydrochloride [Compound (349)].

Workup

  1. temperatureice-cooling
  2. concentrationThe reaction mixture was concentrated under reduced pressure
  3. washthe deposited crystal was washed with diethyl ether
  4. customdried

Sources & evidence

ORD record
ord-550b30526e2b4e2a9c07f06e5edc5cfc
Source dataset
uspto-grants-1987_11
Patent number
US04709052

Reaction notes

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