HRID248030

反应详情

EQUATION

反应方程式

HRID 248030 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The title compound is prepared by the procedure of Example 27, using 2.9 g of product from Example 132, 1.3 g of product from Example 12, 0.433 g of 50% sodium hydride and 60 ml of dry tetrahydrofuran. The residue is purified by chromatography to give 1.74 g of the desired product as a yellow oil.

WORKUP

后处理

  1. customThe title compound is prepared by the procedure of Example 27
  2. customThe residue is purified by chromatography