反应详情

温度

60 °C

Combine N-[methoxy]-N-[methyl]3-cyclopentylamino-4-nitrobenzamide (2.0 g, 6.82 mmol), ammonium formate (2.1 g, 34.1 mmol), and 0.36 g (3.41 mmol) Pd(C) in ethanol (25 mL). Heat the mixture to 60° C. and stir for two hours. Cool to room temperature and filter through a pad of celite. Concentrate the filtrate under reduced pressure to provide the desired compound (1.79 g).

1. temperatureCool to room temperature
2. filtrationfilter through a pad of celite
3. concentrationConcentrate the filtrate under reduced pressure