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HRID251076

反应详情

EQUATION

反应方程式

HRID 251076 的结构方程式

REACTANTS

反应物

2
结构：CC(C)(C)OC(=O)NCCCCN
HCID4351

未命名化合物

结构：CC(=O)c1ccccn1
HCID14286

1-(2-Pyridyl)-1-ethanone

C7H7NO

PRODUCTS

生成物

1
结构：CC(NCCCCNC(=O)OC(C)(C)C)c1ccccn1
HCID67272354

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

结构：CC(=O)O[BH-](OC(C)=O)OC(C)=O.[Na+]
溶剂HCID5049666

Sodium triacetoxyborohydride

C6H10BNaO6

PROCEDURE

实验过程

Using General Procedure B, (4-aminobutyl)-carbamic acid tert-butyl ester and 2-acetylpyridine in CH2Cl2 and NaBH(OAc)3 were reacted to obtain [4-(1-pyridin-2-ylethylamino)-butyl]-carbamic acid tert-butyl ester as a light brown oil.

WORKUP

后处理

  1. customwere reacted