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HRID251117

反应详情

EQUATION

反应方程式

HRID 251117 的结构方程式

REACTANTS

反应物

3
结构：CC(N)c1ccccn1
HCID541877

1-(2-Pyridinyl)ethanamine

C7H10N2

结构：CC(C)(C)OC(=O)N1CCC(=O)CC1
HCID735900

1-Boc-4-piperidone

C10H17NO3

结构：CC(=O)O[BH-](OC(C)=O)OC(C)=O.[Na+]
HCID5049666

Sodium triacetoxyborohydride

C6H10BNaO6

PRODUCTS

生成物

1
结构：CC(NC1CCN(C(=O)OC(C)(C)C)CC1)c1ccccn1
HCID60137113

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl
溶剂HCID6344

Dichloromethane

CH2Cl2

PROCEDURE

实验过程

Using General Procedure B: Reaction of 1-Pyridin-2-yl-ethylamine and 1-Boc-4-piperidone with NaBH(OAc)3 in CH2Cl2 gave 4-(1-Pyridin-2-yl-ethylamino)-piperidine-1-carboxylic acid tert-butyl ester as a colorless oil.