HRID255222

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID61147

Acetyl bromide, 2-bromo-

C2H2Br2O

HCID351840

2-Amino-4-Bromophenol

C6H6BrNO

HCID10654813

3-Oxo-3,4-dihydro-2H-1,4-benzoxazine-6-carbonitrile

C9H6N2O2

PRODUCTS

生成物

HCID16218142

6-Bromo-2H-1,4-benzoxazin-3(4H)-one

C8H6BrNO2

PROCEDURE

实验过程

2-Amino-4-bromophenol (2.1 g, 11 mmol) and bromo acetyl bromide (1.4 mL, 16.5 mmol) were reacted according to the procedure for Intermediate 60 to afford product as a solid, 2.1 g (85%).

WORKUP

后处理

customto afford product as a solid, 2.1 g (85%)