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HRID25610

反应详情

EQUATION

反应方程式

HRID 25610 的结构方程式

REACTANTS

反应物

4
结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：C1CCNCC1
HCID8082

Piperidine

C5H11N

结构：O=C(Cl)Oc1ccc(Cl)cc1
HCID139059

4-Chlorophenyl chloroformate

C7H4Cl2O2

结构：CN[C@H]1CC[C@H](CCCCCOS(C)(=O)=O)CC1
HCID178484796

未命名化合物

PRODUCTS

生成物

1
结构：CN(C(=O)Oc1ccc(Cl)cc1)[C@H]1CC[C@H](CCCCCN2CCCCC2)CC1
HCID178485959

未命名化合物

PROCEDURE

实验过程

In analogy to examples 29.10 and 29.11, trans-Methansulfonic acid 5-(4-methyl amino-cyclohexyl)-pentyl ester.trifluoroacetic acid salt and 4-chlorophenyl chloroformate were reacted, followed by treatment with piperidine to give trans-Methyl-[4-(5-piperidin-1-yl-pentyl)-cyclohexyl]-carbamic acid 4-chloro-phenyl ester, MS: 421 (MH+, 1Cl).