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HRID25611

反应详情

EQUATION

反应方程式

HRID 25611 的结构方程式

REACTANTS

反应物

4
结构：O=C(O)C(F)(F)F
HCID6422

未命名化合物

结构：CN1CCNCC1
HCID53167

1-Methylpiperazine

C5H12N2

结构：O=C(Cl)Oc1ccc(Cl)cc1
HCID139059

4-Chlorophenyl chloroformate

C7H4Cl2O2

结构：CN[C@H]1CC[C@H](CCCCCOS(C)(=O)=O)CC1
HCID178484796

未命名化合物

PRODUCTS

生成物

1
结构：CN1CCN(CCCCC[C@H]2CC[C@H](N(C)C(=O)Oc3ccc(Cl)cc3)CC2)CC1
HCID178480863

未命名化合物

PROCEDURE

实验过程

In analogy to examples 29.10 and 29.11, trans-Methansulfonic acid 5-(4-methyl amino-cyclohexyl)-pentyl ester.trifluoroacetic acid salt and 4-chlorophenyl chloroformate were reacted, followed by treatment with N-methyl-piperazine to give trans-Methyl-{4-[5-(4-methyl-piperazin-1-yl)-pentyl]-cyclohexyl}-carbamic acid 4-chloro-phenyl ester, MS: 436 (MH+, 1Cl).