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HRID25756

反应详情

EQUATION

反应方程式

HRID 25756 的结构方程式

REACTANTS

反应物

4
结构：C=CCO
HCID7858

Allyl alcohol

C3H6O

结构：C[Si](C)(C)[N-][Si](C)(C)C.[Na+]
HCID2724254

Sodium bis(trimethylsilyl)amide

C6H18NNaSi2

结构：C=CCOCC1=CC(C)(C)Nc2ccc(-c3ccccc3OC)cc21
HCID10314903

未命名化合物

结构：COc1ccccc1-c1ccc2c(c1)C(CBr)=CC(C)(C)N2
HCID22566535

未命名化合物

PRODUCTS

生成物

1
结构：COc1ccccc1-c1ccc2c(c1)C(CNc1ccccc1)=CC(C)(C)N2
HCID10406857

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1
溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

4-Allyloxymethyl-6-(2-methoxyphenyl)-2,2-dimethyl-1,2-dihydroquinoline 40 mg of 4-bromomethyl-6-(2-methoxyphenyl)-2,2-dimethyl-1,2-dihydroquinoline, 44 μL of allyl alcohol, and 4 mL of 1 M solution of sodium bis(trimethylsilyl)amide in THF reacted to give 4.5 mg of the title compound as a foam.