HRID258356

反应详情

EQUATION

反应方程式

HRID 258356 的结构方程式

PROCEDURE

实验过程

1-Amino-2-carboxy-4-(3'-amino-4'-sulfophenylthio)anthraquinone (9.4 parts) and cyanuric chloride (3.7 parts) were subjected a to condensation reaction in an aqueous medium in a usual manner, followed by a condensation reaction with 1-aminobenzene-3-β-sulfatoethylsulfone (5.6 parts) at 20° to 40° C. under a weak acid condition. Thereafter, salting out of the reaction mixture with sodium chloride gave an anthraquinone compound of the following formula (free acid form). ##STR270##

WORKUP

后处理

  1. customto condensation reaction in an aqueous medium in a usual manner