Hydrochloric Acid → HCID 178480762, compound

HRID 258665Notes

Reaction equation

HRID 258665 reaction equation
[Cl:1][C:2]1[C:19]2[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=2)[N:13]=[C:4]([C:5]([NH:7][C:8]2[NH:12][N:11]=[N:10][N:9]=2)=[O:6])[CH:3]=1.[CH3:20][N:21]1[CH2:26][CH2:25][NH:24][CH2:23][CH2:22]1.[ClH:27]>O>[ClH:1].[ClH:27].[ClH:1].[CH3:20][N:21]1[CH2:26][CH2:25][N:24]([C:2]2[C:19]3[C:14](=[CH:15][CH:16]=[CH:17][CH:18]=3)[N:13]=[C:4]([C:5]([NH:7][C:8]3[NH:12][N:11]=[N:10][N:9]=3)=[O:6])[CH:3]=2)[CH2:23][CH2:22]1

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 531671-MethylpiperazineHCID 178522680HCID 178522680, compound

Product 1

HCID 178480762HCID 178480762, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent2×

Procedure

4-Chloro-N(1H-tetrazol-5-yl)quinaldamide (0.6 g), N-methylpiperazine (5 ml) and water (1 ml) were heated on a steam bath for 18 hours. Water (5 ml) and dilute hydrochloric acid were added to pH 1 and the solid was collected and washed with 0.1 N hydrochloric acid and dried, m.p. 215° (d).

Workup

  1. customthe solid was collected
  2. washwashed with 0.1 N hydrochloric acid
  3. customdried

Sources & evidence

ORD record
ord-5c69dfa5d9bd47e088fb69b4c5755d32
Source dataset
uspto-grants-1977_07
Patent number
US04034075

Reaction notes

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