反应详情

One mole of n-nonadecyl-n-tetradecyl-n-decylcarbinol is added to 0.2 liters of methylene chloride and 0.32 moles calcium chloride. Approximately 1.5 moles of HCl gas is slowly bubbled through the solution. The product mixture is then washed with 1 liter of a 10% sodium carbonate solution. The organic layer is dried with magnesium sulfate and the methylene chloride is evaporated off to give n-nonadecyl-n-tetradecyl-n-decylmethylchloride.

1. washThe product mixture is then washed with 1 liter of a 10% sodium carbonate solution
2. dry with materialThe organic layer is dried with magnesium sulfate
3. customthe methylene chloride is evaporated off