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HRID25927

反应详情

EQUATION

反应方程式

HRID 25927 的结构方程式

REACTANTS

反应物

3
结构：O=C(Cl)Cl
HCID6371

Phosgene

CCl2O

结构：C[Si](C)(C)Cl
HCID6397

Chlorotrimethylsilane

C3H9ClSi

结构：CC1=CCC(=NN2CCNC2=O)O1
HCID70569531

未命名化合物

PRODUCTS

生成物

1
结构：CC1=CCC(=NN2CCN(C(=O)Cl)C2=O)O1
HCID86736435

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCN(CC)CC
溶剂HCID8471

Triethylamine

C6H15N

PROCEDURE

实验过程

50.0 pts. by wt. of 1-(5-methylfurylideneamino)-2-oxo-imidazolidine, 84.3 pts. by wt. of triethylamine, 84.0 pts. by wt. of chlorotrimethylsilane and 51.4 pts. by wt. of phosgene are reacted as in Example 1.2. After recrystallisation from acetonitrile, 50.7 pts. by wt. of 1-chlorocarbonyl-2-oxo-3-(5-methylfurylideneamino)-imidazolidine of dec. pt. 180°-186° C. are obtained.

WORKUP

后处理

  1. customAfter recrystallisation from acetonitrile, 50.7 pts