HRID260494

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：NC(=O)c1[nH]c2ccc(Cl)cc2c1S(=O)(=O)c1ccccc1

HCID454844

3-Benzenesulfonyl-5-chloroindole-2-carboxamide

C15H11ClN2O3S

结构：CCC[N+](CC)(CC)S(=O)(=O)NC(=O)O.[OH-]

HCID86749577

未命名化合物

PRODUCTS

生成物

结构：N#Cc1[nH]c2ccc(Cl)cc2c1S(=O)(=O)c1ccccc1

HCID22401514

3-(Benzenesulfonyl)-5-chloro-1H-indole-2-carbonitrile

C15H9ClN2O2S

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID8028

Tetrahydrofuran

C4H8O

PROCEDURE

实验过程

5-Chloro-3-phenylsulfonylindole-2-carboxamide reacts with methyl (carboxysulfamoyl)triethylammonium hydroxide inner salt (Burgess reagent) in tetrahydrofuran (THF) solvent as described by D. A. Claremon and B. T. Phillips (Tetrahedron Lett., 29, 2155 (1988)) to provide the title compound.