HRID263656

反应详情

EQUATION

反应方程式

HRID 263656 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

Since the actual yield and the actual Act[O] were 38.0 g and 7.31%, respectively, the uncorrected yield was 77.2% and the yield corrected for Act[O] (i.e., the corrected yield) was 79.1%. The higher than expected Act[O] indicated that t-butyl hydroperoxide was somewhat more reactive towards fumaryl chloride than the n-butanol was. The first peroxyfumarate composition (Preparation 1) was found to have a half-life of 19.0 hours at 100° C. in alpha-methylstyrene based on conventional determination procedures.

WORKUP

后处理

  1. customSince the actual yield
  2. customthe corrected yield)
  3. customa half-life of 19.0 hours
  4. customat 100° C.