HRID263656
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
Since the actual yield and the actual Act[O] were 38.0 g and 7.31%, respectively, the uncorrected yield was 77.2% and the yield corrected for Act[O] (i.e., the corrected yield) was 79.1%. The higher than expected Act[O] indicated that t-butyl hydroperoxide was somewhat more reactive towards fumaryl chloride than the n-butanol was. The first peroxyfumarate composition (Preparation 1) was found to have a half-life of 19.0 hours at 100° C. in alpha-methylstyrene based on conventional determination procedures.
WORKUP
后处理
- customSince the actual yield
- customthe corrected yield)
- customa half-life of 19.0 hours
- customat 100° C.