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HRID264737

反应详情

EQUATION

反应方程式

HRID 264737 的结构方程式

REACTANTS

反应物

3
结构：Nc1ccn([C@@H]2O[C@H](CO)[C@@H](O)[C@H]2O)c(=O)n1
HCID6175

Cytidine

C9H13N3O5

结构：CCCCCCCCCI
HCID20275

1-Iodononane

C9H19I

结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

PRODUCTS

生成物

1
结构：CCCCCCCCCO[C@@H]1[C@H](O)[C@@H](CO)O[C@H]1n1ccc(N)nc1=O
HCID22868393

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

N,N-Dimethylformamide

C3H7NO

PROCEDURE

实验过程

Cytidine (10.1 g, 0.0415 mol), sodium hydride (2.0 g, 1.2 eq), iodononane (9.8 ml, 1.2 eq.) in DMF (100 ml) were reacted as per the procedure of Example 71, Step 1 to yield the 2' and 3' isomers as a sticky foam (11.6 g).