huagongshe.com
HRID264960

反应详情

EQUATION

反应方程式

HRID 264960 反应方程式

REACTANTS

反应物

2
Hydrochloric Acid 分子结构式
HCID313

Hydrochloric Acid

ClH

HCID 10944665 分子结构式
HCID10944665

未命名化合物

PRODUCTS

产物

1
N,N-Dimethyl-L-valinamide--hydrogen chloride (1/1) 分子结构式
HCID56831841

N,N-Dimethyl-L-valinamide--hydrogen chloride (1/1)

C7H17ClN2O

AUXILIARIES

试剂、催化剂与溶剂

1
1,4-Dioxane 分子结构式
溶剂HCID31275

1,4-Dioxane

C4H8O2

CONDITIONS

反应条件

温度
0 °C

PROCEDURE

实验过程

0.85 g of 2(S)-tert-butoxycarbonylamino-3-methylbutanoic acid (N,N-dimethyl)amide is dissolved in 10 ml of 4N hydrochloric acid in dioxane at 0° C. and stirred for 7 hours at 0° C. The reaction mixture is lyophilised and the title compound is obtained: Rf (ethyl acetate/methanol/conc. ammonia=80:15:5)=0.23.