反应详情

A mixture of 40.5 g. (0.1 moles) of ethyl α-bromo-2'-chloro-4-biphenylylacetate and 150 g. of sodium iodide in 1 liter of anhydrous acetone is refluxed for 4 hours. The reaction mixture is then evaporated to dryness and extracted with ether. The ether is then washed with water, dried and evaporated to dryness to obtain ethyl α-iodo-2'-chloro-4-biphenylylacetate.

1. additionA mixture of 40.5 g
2. customThe reaction mixture is then evaporated to dryness
3. extractionextracted with ether
4. washThe ether is then washed with water
5. customdried
6. customevaporated to dryness