3-Phenylprop-2-En-1-Ol → HCID 316618, compound

HRID 267672Notes

Reaction equation

[CH2:1]([OH:10])[CH:2]=[CH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1.[CH2:11](I)[CH3:12]>>[CH2:1]([O:10][CH2:11][CH3:12])[CH:2]=[CH:3][C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1

Participants

Reactant 2

HCID 3083-Phenylprop-2-En-1-Ol

HCID 6340Iodoethane

Product 1

HCID 316618HCID 316618, compound

Procedure

Reaction of cinnamyl alcohol with ethyl iodide was carried out in the same manner as described in Example I. The analytical data supported the assigned structure and GC analysis indicated a purity of 99+%: λmaxCCl4 6.66, 6.87, 7.25, 8.75-9.1, 10.35 and 14.45 μ.

Sources & evidence

ORD record: ord-a5e6b39110194ea6a893a99041f78fdc
Source dataset: uspto-grants-1976_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03943943

Reaction notes

Loading…