3,4-Dimethoxyaniline → HCID 4333080, compound

HRID 267878Notes

Reaction equation

HRID 267878 reaction equation
[C:1]12([C:11](Cl)=[O:12])[CH2:10][CH:5]3[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]3)[CH2:2]1)[CH2:8]2.[NH2:14][C:15]1[CH:16]=[C:17]([O:23][CH3:24])[C:18]([O:21][CH3:22])=[CH:19][CH:20]=1>C(N(CC)CC)C>[CH3:24][O:23][C:17]1[CH:16]=[C:15]([NH:14][C:11]([C:1]23[CH2:10][CH:5]4[CH2:6][CH:7]([CH2:9][CH:3]([CH2:4]4)[CH2:2]2)[CH2:8]3)=[O:12])[CH:20]=[CH:19][C:18]=1[O:21][CH3:22]

Participants

4

Reactant 2

HCID 227703,4-DimethoxyanilineHCID 989151-Adamantanecarbonyl chloride

Product 1

HCID 4333080HCID 4333080, compound

Reagents, catalysts & solvents 1

HCID 8471TriethylamineSolvent

Procedure

Subject 1.35 g. (6.8 mmoles) of adamantane carboxylic acid chloride, 1.0 g. (6.5 mmoles) of 4-amino veratrole and 4.0 ml. of triethylamine to the process of Example 11 and obtain thereby the title product, m.p. 224°-226°C.

Sources & evidence

ORD record
ord-86043e750093424fb3e8949aa661a9dd
Source dataset
uspto-grants-1976_03
Patent number
US03944675

Reaction notes

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