HRID267914

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID12025

2-Pyrrolidinone

C4H7NO

HCID24813

Phosphoric trichloride

Cl3OP

HCID74490

Methyl phenothiazin-2-yl ether

C13H11NOS

PRODUCTS

生成物

结构：COc1ccc2c(c1)N(C1=CCCN1C1=NCCC1)c1ccccc1S2

HCID12799392

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

溶剂HCID11

1,2-Dichloroethane

C2H4Cl2

PROCEDURE

实验过程

Reaction of 2-methoxyphenothiazine, 2-pyrrolidinone and phosphorus oxychloride in 1,2-dichloroethane according to the procedure of Example 1 affords 2-METHOXY-10-[1-(1-PYRROLIN-2-YL)-2PYRROLIN-2-YL]PHENOTHIAZINE free base, m.p. 151°-153° C. (corr.), from isopropyl alcohol.