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HRID273023

反应详情

EQUATION

反应方程式

HRID 273023 的结构方程式

REACTANTS

反应物

4
结构：[I-].[K+]
HCID4875

Potassium iodide

IK

结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：CC(C)(C)OC(=O)N(CCCl)CCCl
HCID11230235

tert-Butyl bis(2-chloroethyl)carbamate

C9H17Cl2NO2

结构：N#CCc1ccc(OCCCN2CCCC2)cc1
HCID23091635

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCC(C#N)(c2ccc(OCCCN3CCCC3)cc2)CC1
HCID68578770

未命名化合物

收率 53%

PROCEDURE

实验过程

The title compound (1.8 g, 53%) was prepared using [4-(3-pyrrolidin-1-ylpropoxy)phenyl]acetonitrile, tert-butyl bis(2-chloroethyl)carbamate, sodium hydride and potassium iodide similarly to the procedure used for intermediate 56. LRMS APCI+ m/z 414 [MH]+ and m/z 245 [SMH]+.