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HRID275376

反应详情

EQUATION

反应方程式

HRID 275376 的结构方程式

REACTANTS

反应物

2
结构：N#Cc1ccc(O)cc1
HCID13019

4-Hydroxybenzonitrile

C7H5NO

结构：CCCc1c(CCl)ccc(C(C)=O)c1O
HCID13781022

未命名化合物

PRODUCTS

生成物

1
结构：CCCc1c(COc2ccc(C#N)cc2)ccc(C(C)=O)c1O
HCID13781030

未命名化合物

PROCEDURE

实验过程

The title nitrile intermediate was prepared from 18.12 g. of 4-acetyl-3-hydroxy-2-propylbenzyl chloride and 35.7 g. of 4-cyanophenol following the general procedure of Example 1. Crystallization from ethanol/water provided 19.0 g. of the desired intermediate, m.p. 102°-103° C.

WORKUP

后处理

  1. customCrystallization from ethanol/water
  2. customprovided 19.0 g