Hydrochloric Acid → HCID 22628259, compound

HRID 278589Notes

Reaction equation

HRID 278589 reaction equation
[CH3:1][N:2]([CH2:4][C:5]1[CH:31]=[CH:30][C:8]([C:9]([N:11]2[CH2:16][CH2:15][N:14]([S:17]([C:20]3[CH:29]=[CH:28][C:27]4[C:22](=[CH:23][CH:24]=[CH:25][CH:26]=4)[CH:21]=3)(=[O:19])=[O:18])[CH2:13][CH2:12]2)=[O:10])=[CH:7][CH:6]=1)[CH3:3].[ClH:32]>C(OCC)(=O)C>[ClH:32].[CH3:3][N:2]([CH2:4][C:5]1[CH:31]=[CH:30][C:8]([C:9]([N:11]2[CH2:12][CH2:13][N:14]([S:17]([C:20]3[CH:29]=[CH:28][C:27]4[C:22](=[CH:23][CH:24]=[CH:25][CH:26]=4)[CH:21]=3)(=[O:18])=[O:19])[CH2:15][CH2:16]2)=[O:10])=[CH:7][CH:6]=1)[CH3:1]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 22628156HCID 22628156, compound

Product 1

HCID 22628259HCID 22628259, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

To 1-(4-dimethylaminomethylbenzoyl)-4-(2-naphthalenesulfonyl)piperazine (42 mg) was added 4 N hydrochloric acid in ethyl acetate solution (1 ml), and the precipitated hydrochlorides were filtered to give the title compound (40 mg).

Workup

  1. filtrationthe precipitated hydrochlorides were filtered

Sources & evidence

ORD record
ord-5542cb54c5a840acbf90a299a4658cd7
Source dataset
uspto-grants-2002_03
Patent number
US06359134B1

Reaction notes

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