Hydrochloric Acid → HCID 22628160, compound

HRID 278591Notes

Reaction equation

HRID 278591 reaction equation
[CH:1]([N:4]([CH2:8][C:9]1[CH:10]=[C:11]([CH:33]=[CH:34][CH:35]=1)[C:12]([N:14]1[CH2:19][CH2:18][N:17]([S:20]([C:23]2[CH:32]=[CH:31][C:30]3[C:25](=[CH:26][CH:27]=[CH:28][CH:29]=3)[CH:24]=2)(=[O:22])=[O:21])[CH2:16][CH2:15]1)=[O:13])[CH:5]([CH3:7])[CH3:6])([CH3:3])[CH3:2].[ClH:36]>C(OCC)(=O)C>[ClH:36].[CH:1]([N:4]([CH2:8][C:9]1[CH:10]=[C:11]([CH:33]=[CH:34][CH:35]=1)[C:12]([N:14]1[CH2:19][CH2:18][N:17]([S:20]([C:23]2[CH:32]=[CH:31][C:30]3[C:25](=[CH:26][CH:27]=[CH:28][CH:29]=3)[CH:24]=2)(=[O:22])=[O:21])[CH2:16][CH2:15]1)=[O:13])[CH:5]([CH3:7])[CH3:6])([CH3:2])[CH3:3]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 22628111HCID 22628111, compound

Product 1

HCID 22628160HCID 22628160, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

To 1-(3-diisopropylaminomethylbenzoyl)-4-(2-naphthalenesulfonyl)piperazine (215 mg) was added 4 N hydrochloric acid in ethyl acetate solution (5 ml), and the precipitated hydrochlorides were filtered to give the title compound (219 mg).

Workup

  1. filtrationthe precipitated hydrochlorides were filtered

Sources & evidence

ORD record
ord-2634814780f4426f800b5a8e7573c380
Source dataset
uspto-grants-2002_03
Patent number
US06359134B1

Reaction notes

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