Hydrochloric Acid → HCID 22628036, compound

HRID 278594Notes

Reaction equation

HRID 278594 reaction equation
[CH:1]([N:4]([CH2:8][C:9]1[CH:35]=[CH:34][C:12]([C:13]([N:15]2[CH2:20][CH2:19][N:18]([S:21]([C:24]3[C:33]4[C:28](=[CH:29][CH:30]=[CH:31][CH:32]=4)[CH:27]=[CH:26][CH:25]=3)(=[O:23])=[O:22])[CH2:17][CH2:16]2)=[O:14])=[CH:11][CH:10]=1)[CH:5]([CH3:7])[CH3:6])([CH3:3])[CH3:2].[ClH:36]>C(OCC)(=O)C>[ClH:36].[CH:1]([N:4]([CH2:8][C:9]1[CH:35]=[CH:34][C:12]([C:13]([N:15]2[CH2:16][CH2:17][N:18]([S:21]([C:24]3[C:33]4[C:28](=[CH:29][CH:30]=[CH:31][CH:32]=4)[CH:27]=[CH:26][CH:25]=3)(=[O:22])=[O:23])[CH2:19][CH2:20]2)=[O:14])=[CH:11][CH:10]=1)[CH:5]([CH3:7])[CH3:6])([CH3:2])[CH3:3]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 22627993HCID 22627993, compound

Product 1

HCID 22628036HCID 22628036, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

To 1-(4-diisopropylaminomethylbenzoyl)-4-(1-naphthalenesulfonyl)piperazine (181 mg) was added 4 N hydrochloric acid in ethyl acetate solution (5 ml), and the precipitated hydrochlorides were filtered to give the title compound (180 mg).

Workup

  1. filtrationthe precipitated hydrochlorides were filtered

Sources & evidence

ORD record
ord-f261e02d11cf4a749cc18c970e114dfb
Source dataset
uspto-grants-2002_03
Patent number
US06359134B1

Reaction notes

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