huagongshe.com
HRID279704

反应详情

EQUATION

反应方程式

HRID 279704 的结构方程式

REACTANTS

反应物

3
结构：[Li+].[OH-]
HCID3939

Lithium hydroxide anhydrous

HLiO

结构：COC(=O)[C@@H](N)Cc1c[nH]c2ccccc12.Cl
HCID2734891

Methyl tryptophanate hydrochloride

C12H15ClN2O2

结构：Cc1ccc(S(=O)(=O)N2CCC[C@H]2C(=O)O)cc1.O
HCID69463844

未命名化合物

PRODUCTS

生成物

1
结构：Cc1ccc(S(=O)(=O)N2CCC[C@H]2C(=O)N[C@@H](Cc2c[nH]c3ccccc23)C(=O)O)cc1
HCID54463657

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：C1CCOC1.O
溶剂HCID21881883

Oxolane--water (1/1)

C4H10O2

PROCEDURE

实验过程

N-(Toluene-4-sulfonyl)-L-proline hydrate was coupled to L-tryptophan methyl ester hydrochloride using the procedure described in Method 3. The title compound was prepared via hydrolysis of the methyl ester using LiOH in THF/water.