Ammonium → 4-(Benzyloxycarbonylamino)cyclohexylidenemethyl methyl ether

HRID 282906Notes

Reaction equation

HRID 282906 reaction equation
[CH2:24]([Li:25])[CH2:26][CH2:27][CH3:28].[CH2:29]([c:30]1[cH:31][cH:32][cH:33][cH:34][cH:35]1)[O:36][C:37](=[O:38])[NH:39][CH:40]1[CH2:41][CH2:42][C:43](=[O:46])[CH2:44][CH2:45]1.[CH3:2][O:3][CH2:4][P+:5]([c:6]1[cH:7][cH:8][cH:9][cH:10][cH:11]1)([c:12]1[cH:13][cH:14][cH:15][cH:16][cH:17]1)[c:18]1[cH:19][cH:20][cH:21][cH:22][cH:23]1.[CH3:49][CH2:50][CH2:51][CH2:52][CH2:53][CH3:54].[Cl-:1].[Cl-:47].[NH4+:48].[O:55]1[CH2:56][CH2:57][CH2:58][CH2:59]1>>[CH3:2][O:3][CH:4]=[C:43]1[CH2:42][CH2:41][CH:40]([NH:39][C:37]([O:36][CH2:29][c:30]2[cH:31][cH:32][cH:33][cH:34][cH:35]2)=[O:38])[CH2:45][CH2:44]1

Participants

8

Reactant 7

HCID 223AmmoniumHCID 312Chloride2×HCID 8028TetrahydrofuranHCID 8058HexaneHCID 2723799(Methoxymethyl)triphenylphosphonium chlorideHCID 14615292Benzyl (4-oxocyclohexyl)carbamateHCID 178418339Butyllithium

Product 1

HCID 189194024-(Benzyloxycarbonylamino)cyclohexylidenemethyl methyl ether

Sources & evidence

ORD record
ord-c8da948007254055b697dda90f5838e6
Source dataset
Training data from https://doi.org/10.1039/C8SC04228D (8/10)

Reaction notes

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