反应详情

In a 100-cm3 flask, the 3-(7-methoxy-1-naphthyl)propyl mesylate obtained in stage D is dissolved in DMSO. KCN is added and the mixture is brought to reflux for 2 h. It is allowed to cool. It is poured into a water/ice mixture. The resulting mixture is extracted with ether. The organic phase is washed with water, dried over CaCl2 and evaporated. The product obtained is recrystallized.

1. temperatureto reflux for 2 h
2. temperatureto cool
3. extractionThe resulting mixture is extracted with ether
4. washThe organic phase is washed with water
5. dry with materialdried over CaCl2
6. customevaporated
7. customThe product obtained
8. customis recrystallized